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International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators 4-8 May 2009 Vienna Energy Monitoring Device for Electron Beam Facilities M. Lavalle 1 , P.G. Fuochi 1 , A. Martelli 1 , U. Corda 1 , A. Kovács 2 , K. Mehta 3 , F. Kuntz 4 , S. Plumeri 4 1 CNR-ISOF, Via P. Gobetti 101, I-40129 Bologna, Italy 2 Institute of Isotopes, HAS, P.O.Box 77, H-1525 Budapest, Hungary 3 Brünner Strasse 133-3-29, Vienna, A-1210, Austria 4 Aérial, Parc d'Innovation Rue Laurent Fries F-67400 Illkirch, France

Energy Monitoring Device for Electron Beam Facilities

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Page 1: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Energy Monitoring Device for Electron Beam Facilities

M. Lavalle1, P.G. Fuochi1, A. Martelli1, U. Corda1, A. Kovács2, K. Mehta3, F. Kuntz4, S. Plumeri4

1 CNR-ISOF, Via P. Gobetti 101, I-40129 Bologna, Italy

2 Institute of Isotopes, HAS, P.O.Box 77, H-1525 Budapest, Hungary

3 Brünner Strasse 133-3-29, Vienna, A-1210, Austria

4 Aérial, Parc d'Innovation Rue Laurent Fries F-67400 Illkirch, France

Page 2: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Introduction

The electron beam energy in commercial radiation processing is one of the critical parameters for quality assurance and quality control since it determines the size of the product box that can be processed and a variation of the energy affects the absorbed dose distribution in the product under irradiation.

Standards procedures require that the beam energy be:

- determined during the facility qualification;

- monitored and controlled during routine irradiation.

Page 3: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Examples of dose distribution in uniform material:

10 MeV

9.8 MeV

Single side irradiation(water, 5 cm)

Double side irradiation(water, 9 cm)

Simulations obtained with the software ModeRTL, Version 2.6.

Page 4: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

0 2 4 6 8 10 120.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

1.6

Rp

R50

Do

se, a.u

.

Depth in Al, mm

Amongst different methods for measuring the electron beam energy, the study of the depth-dose distribution in a homogeneous reference material is the widely used technique.

Empirical energy-range relations for

mean electron energy:Ea = (2.33 MeV•cm-1) • (R50 cm)(5 MeV ≤ Ea ≤ 35 MeV, in H2O phantom)

most probale electron energy:Ep = (5.09 MeV•cm-1) • (Rp cm) +

0.20 MeV(5 MeV ≤ Ep ≤ 25 MeV, in Al phantom)

(examples from ICRU, 1984. Radiation dosimetry: Electron beams with energy between 1 and 50 MeV,Report No. 35. International Commission on Radiation Units and Measurements, Bethesda, MD, USA.)

Page 5: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

0 5 10 15 20

500

0

-500

-1000

-1500

-2000

-2500

-3000

-3500

50

0

-50

-100

-150

-200

-250

-300

-350

-400

-450

inte

gra

l co

llecte

d c

harg

e, 10

-8C

Depth in Al, mm

dif

fere

nti

al co

llecte

d c

harg

e, 10

-8C

Another possible method, which is the subject of this work, is the study of the influence of the electron beam energy on the charge distribution with depth in homogeneous absorbers.

Page 6: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

0 1 2 3 4 5 6 7-0.3

-0.2

-0.1

0.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

5 MeV

ISOF 10 MeV

e- c

m2/(

g•i

ncid

ent

ele

ctr

on

s)

g/cm2

Differential charge-deposition distributions in aluminium for ISOF LINAC beam (experimental, 8 MeV), and for 5 and 10 MeV mono-energetic beams (calculated, from Andreo, P., Ito, R., Tabata, T., 1992. Tables of charge- and energy-deposition distributions in elemental materials irradiated by plane-parallel electron beams with energies between 0.1 and 100 MeV, Report ISSN 0917-8015, Res. Inst. Adv. Sci. Tech., Univ. Osaka Pref., Japan.).

Page 7: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

0 5 10 15 20 250

-200

-400

Ep

mm Al

diffe

rential charg

e (

10

-8C

)

0 5 10 15 20 250

-200

-400 Ep" < E

p

Ep

mm Al

diffe

rential charg

e (

10

-8C

)

0 5 10 15 20 250

-200

-400

Ep' > E

p

Ep

mm Al

diffe

rential charg

e (

10

-8C

)

The basic idea:

Page 8: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

The first device:K. Mehta, J. Barnard, W. Stanley and A. UngerExperience with e-beam process dosimetry at the WhiteshellIrradiator

International Symposium on High Dose Dosimetry for Radiation ProcessingVienna 5-9 November 1990

Proceedings Series STI/PUB/846, 1991, ISBN 92-0-010291-3, 28 June 1991, 451-458.

two 1.25 cm thick Al plates

Page 9: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

The actual device:

Aluminium cage 140 mm x 140 mm x 100 mm (h) 10 mm thick

Front plate 2, 5 or 12 mm

Back plate 25 mm

100 mm

Ceramic pillars

BNC connectors to A-meters

e-

5 mm air gap

To ground

Page 10: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Definition of the “energy ratio” (E.R.):

=+

1

1 2

I

E.R.I I

where:

I1 is the current from the front plate

I2 is the current from the back plate

Page 11: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Location Beam characteristics

Thickness of thefront absorber

(the back absorberwas always 25 mm)

Energy rangeMeV

ISOF-CNRBologna (Italy)

ResearchL-band LINAC0.2 – 5 µs pulses at 50 Hzenergy varied changing thepulse length and the beam current

12 mm 6.5 – 11.5

Institute of IsotopesBudapest (Hungary)

ResearchTesla LPR-4 LINAC2.6 µs pulses at 50 Hzenergy varied changingthe beam current

5 mm 4 – 6

FE-MA Co. Ltd.Budapest (Hungary)

CommercialLUE-8 LINAC3.6 µs pulses at 50 Hzbeam scanned at 5 Hzenergy varied changing the magnetronhigh voltage and the beam current

5 mm 4 – 6.5

Gambro-DascoMedolla (Italy)

CommercialRhodotron TT-100“continuous” beam, 0.5 – 2.7 mAbeam scanned at 100 Hzenergy does not vary

12 mm 10

The previous tests

Page 12: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Several measuring techniques adopted:

- measurement of the charge deposited into the absorbers through the integration of the current for a fixed time, using digital current integrators (EG&G ORTEC 439) [ISOF, LINAC]

- measurement of the currents using EG&G ORTEC 439, used as current monitor [Gambro Dasco Spa, Rhodotron]

- dedicated measuring instrument realized using an integrated circuit, with ultra low bias and fast slew rate, selected so that its offset voltage and its temperature drift were as low as possible, hardwired in the current amplifier configuration [Institute of Isotopes, LINAC and FE-MA Co. Ltd., LINAC]

Page 13: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1

4 5 6 7 8 9 10 11 12E p , MeV

En

erg

y r

atio

FEMA Co. Ltd., Budapest, LUE-8 LINAC ISOF-CNR, Bologna, Vickers L-band LINAC

Istitute of Isotopes, Budapest, Tesla LPR-4 LINAC Gambro Dasco Spa, Medolla (MO), TT100 Rhodotron

The previous results

Page 14: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Aim of the actual work:

- extension of the method to a lower energy region (around 2 MeV)

- tests on the sensitivity performances of the device

Experimental:

Electron beam source:0.5 - 2.4 MeV; 1 - 125 µA Van De Graaff electron acceleratorAérial (Strasbourg, France)

Energy monitoring device:Thickness of front absorber plate: 2 mmMeasurement of the currents: electrometer Keithley 610B ormultimeter (ITT Metrix MX512)

Energy measurement:Ep: B3 radiochromic film dosimeters placed in within several polystyrene foils (stack technique)

Page 15: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Page 16: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Depth-dose curves in polystyrene (PS).

0

0.2

0.4

0.6

0.8

1

1.2

1.4

1.6

0 0.2 0.4 0.6 0.8 1 1.2 1.4

cm in PS

dose a

.u.

2.4 MeV

2.0 MeV

1.5 MeV

Page 17: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Nominal electronbeam energy*(as set by the highvoltage control)

MeV

Practical electronbeam rangemeasured in PS(ρ = 1.06 g·cm-3)

cm

Practical electronbeam rangescaled to water(ρ = 1 g·cm-3)

cm

Calculatedmost probableenergy Ep

MeV

1.5 0.62 0.64 1.5

2.0 0.86 0.88 2.0

2.4 1.08 1.11 2.4

Nominal electron beam energy vs. the most probable electron beam energy:

*Calibrated during the facility installationusing the technique of foil activation

Page 18: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Response of the energy monitoring device using the electrometer.

0.2

0.3

0.4

0.5

0.6

0.7

0.8

1.4 1.6 1.8 2 2.2 2.4

Electron beam energy, MeV

Energ

y r

atio

Page 19: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Test of the sensitivity of the energy monitoring device;

measurements with electrometer (●) and multimeter (�).

0.250

0.270

0.290

0.310

0.330

0.350

2.14 2.16 2.18 2.2 2.22 2.24 2.26

Electron beam energy, MeV

Energ

y r

atio

Page 20: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Conclusions

The energy monitoring device:

- able to monitor variations in the electron beam in the range of 1.5 - 2.4 MeV (2 mm front absorber)

- sensitivity of at least 40 keV

- robust and immediate response: easy integration in the control system of an electron beam irradiation facility

- the range of possible beam energy can be easily accommodated byproperly selecting the thickness of the two absorber plates

- a variety of techniques can be adopted to measure the currents (or the charges) generated by accumulated electrons in the absorber plates

- for accurate measurements, either an electrometer or a dedicated circuit is needed

Page 21: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Future developments:

integration of a dedicated energy monitoring device, equipped with dedicated electronic, in research or industrial facilities for on-line monitoring of the electron beam energy. (Aérial, Strasbourg)

Page 22: Energy Monitoring Device for Electron Beam Facilities

International Topical Meeting on Nuclear Research Applications and Utilization of Accelerators4-8 May 2009 Vienna

Thank you !

AcknowledgementsThis work was completed within the framework of the Association de Coordination Technique pour l’Industrie Agro-alimentaire (ACTIA) project “Mobilité des Chercheurs” MOB 08.01 and within the framework of the Agreement on Scientific and Technological Cooperation between the National Research Council of Italy and the Hungarian Academy of Sciences.